Multi-scale and Multi-modal Analysis of Metamorphic Rocks Coupling Fluorescence and TXM Techniques

Rocks are commonly polycrystalline systems presenting multi-scale chemical and structural heterogeneities inherited from crystallization processes or successive metamorphic events. Through different applications on metamorphic rocks involving fluorescence microprobes and full-field spectroscopy, one will illustrate how spatially resolved analytical techniques allow rock compositional variations to be related to large-scale geodynamic processes. Those examples also stress the importance of multi-modality instruments with zoom-in capability to study samples from mm to several µm large fields of view, with micrometer down to sub-100 nanometer spatial resolutions. In this perspective, imaging capabilities offered by the new ultra-bright diffraction limited synchrotron sources will be described based on experimental data. At last, the new hard X-ray Transmission X-ray Microscope (TXM) at Sector 32 of the APS at Argonne National Laboratory, performing nano computed tomography with in situ capabilities will be presented. The instrument benefit from several R&D key activities like the fabrication of new zone plates in the framework of the Multi-Bend Achromat Lattice (MBA) upgrade at APS, or the development of powerful tomography reconstruction algorithms able to operate with a limited number of projections.